TY - JOUR
T1 - High-Performance Tungsten Components via Low-Temperature Spray-Dried Powder and Low-Energy SLM
T2 - A Breakthrough for Refractory Metal Additive Manufacturing
AU - Zhang, Yajuan
AU - Wang, Shang
AU - Liu, Xingwei
AU - Sun, Zhe
AU - Liu, Huagang
AU - Huang, Dunhua
N1 - Publisher Copyright:
© 2025 The Author(s). Engineering Reports published by John Wiley & Sons Ltd.
PY - 2025/10
Y1 - 2025/10
N2 - Tungsten's ultrahigh melting point and thermal stress-induced cracking pose significant challenges for additive manufacturing. To address this, we propose a novel strategy combining low-temperature spray drying with optimized heat treatment to fabricate spherical tungsten (W) powders with high sphericity (≥ 95%), narrow particle size distribution (10–50 μm), and excellent flowability (28 s/50 g). Compared to conventional plasma-spheroidized powders, our method reduces production costs and enables selective laser melting (SLM) at remarkably low energy densities (200–600 J/mm3), far below the typical range of 500–1500 J/mm3. Mechanistic analysis reveals that the tailored powder structure suppresses thermal shrinkage cracks by lowering the critical ratio of laser energy density to scanning speed (E/v ≤ 2). At E/v = 1.7 (170 W, 300 mm/s, 0.08 mm spacing), the printed components achieve a relative density of 94.1% (vs. 96% for high-energy SLM) and microhardness of 488 kg/mm2, surpassing commercial cast tungsten (423 kg/mm2). Notably, nanoindentation tests demonstrate exceptional plasticity (indentation work: 0.204 kN·m/m2), comparable to single-crystal tungsten. This work not only establishes a low-cost pathway for refractory metal additive manufacturing but also provides a universal parameter framework (E/v threshold) to mitigate defects in high-melting-point alloys and improves the issues of element evaporation and combustion in additive manufacturing of refractory alloys.
AB - Tungsten's ultrahigh melting point and thermal stress-induced cracking pose significant challenges for additive manufacturing. To address this, we propose a novel strategy combining low-temperature spray drying with optimized heat treatment to fabricate spherical tungsten (W) powders with high sphericity (≥ 95%), narrow particle size distribution (10–50 μm), and excellent flowability (28 s/50 g). Compared to conventional plasma-spheroidized powders, our method reduces production costs and enables selective laser melting (SLM) at remarkably low energy densities (200–600 J/mm3), far below the typical range of 500–1500 J/mm3. Mechanistic analysis reveals that the tailored powder structure suppresses thermal shrinkage cracks by lowering the critical ratio of laser energy density to scanning speed (E/v ≤ 2). At E/v = 1.7 (170 W, 300 mm/s, 0.08 mm spacing), the printed components achieve a relative density of 94.1% (vs. 96% for high-energy SLM) and microhardness of 488 kg/mm2, surpassing commercial cast tungsten (423 kg/mm2). Notably, nanoindentation tests demonstrate exceptional plasticity (indentation work: 0.204 kN·m/m2), comparable to single-crystal tungsten. This work not only establishes a low-cost pathway for refractory metal additive manufacturing but also provides a universal parameter framework (E/v threshold) to mitigate defects in high-melting-point alloys and improves the issues of element evaporation and combustion in additive manufacturing of refractory alloys.
KW - high-sphericity tungsten powder
KW - low-energy-density selective laser melting
KW - low-temperature spray drying
KW - narrow particle size distribution
KW - refractory metal
UR - http://www.scopus.com/pages/publications/105018472982
U2 - 10.1002/eng2.70426
DO - 10.1002/eng2.70426
M3 - Article
AN - SCOPUS:105018472982
SN - 2577-8196
VL - 7
JO - Engineering Reports
JF - Engineering Reports
IS - 10
M1 - e70426
ER -